Hdl Handle:
http://hdl.handle.net/10149/98381
Title:
Sol-gel processing of tellurite powder
Authors:
Weng, L. T. (Luqian); Hodgson, S. N. B. (Simon)
Affiliation:
Loughborough University. Institute of Polymer Technology and Materials Engineering.
Citation:
Weng, L. Q. and Hodgson, S. N. B. (2001) 'Sol-gel processing of tellurite powder', Journal of Materials Science, 36 (20), pp.4955-4959.
Publisher:
Springer Verlag
Journal:
Journal of Materials Science
Issue Date:
15-Oct-2001
URI:
http://hdl.handle.net/10149/98381
DOI:
10.1023/A:1011856824607
Abstract:
Tellurium ethoxide is highly sensitive to moisture in air and water. The hydrolysis and condensation of tellurium ethoxide exposed under different levers of water and moisture are investigated in this work and the hydrolysis products were characterised by infrared spectrometry and X-ray diffraction. The decomposition process of the product of tellurium ethoxide hydrolysed in air was analysed by differential scanning calorimetry and thermogravimetry. This work also studied the influence of sodium component on the phase transformation of the hydrolysis product in the decomposition process and on the morphology of the heat-treated hydrolysis products.
Type:
Article
Language:
en
Keywords:
condensation; decomposition; differential scanning calorimetry; hydrolysis; infrared spectrometers; moisture; phase transitions; powders; refractive index; sol-gels; water; X-ray diffraction analysis
ISSN:
0022-2461; 1573-4803
Rights:
Author can archive post-print (ie final draft post-refereeing). For full details see http://www.sherpa.ac.uk/romeo/ [Accessed 10/05/2010]
Citation Count:
1 [Scopus, 10/05/2010]

Full metadata record

DC FieldValue Language
dc.contributor.authorWeng, L. T. (Luqian)en
dc.contributor.authorHodgson, S. N. B. (Simon)en
dc.date.accessioned2010-05-10T15:31:34Z-
dc.date.available2010-05-10T15:31:34Z-
dc.date.issued2001-10-15-
dc.identifier.citationJournal of Materials Science; 36(20):4955-4959en
dc.identifier.issn0022-2461-
dc.identifier.issn1573-4803-
dc.identifier.doi10.1023/A:1011856824607-
dc.identifier.urihttp://hdl.handle.net/10149/98381-
dc.description.abstractTellurium ethoxide is highly sensitive to moisture in air and water. The hydrolysis and condensation of tellurium ethoxide exposed under different levers of water and moisture are investigated in this work and the hydrolysis products were characterised by infrared spectrometry and X-ray diffraction. The decomposition process of the product of tellurium ethoxide hydrolysed in air was analysed by differential scanning calorimetry and thermogravimetry. This work also studied the influence of sodium component on the phase transformation of the hydrolysis product in the decomposition process and on the morphology of the heat-treated hydrolysis products.en
dc.language.isoenen
dc.publisherSpringer Verlagen
dc.rightsAuthor can archive post-print (ie final draft post-refereeing). For full details see http://www.sherpa.ac.uk/romeo/ [Accessed 10/05/2010]en
dc.subjectcondensationen
dc.subjectdecompositionen
dc.subjectdifferential scanning calorimetryen
dc.subjecthydrolysisen
dc.subjectinfrared spectrometersen
dc.subjectmoistureen
dc.subjectphase transitionsen
dc.subjectpowdersen
dc.subjectrefractive indexen
dc.subjectsol-gelsen
dc.subjectwateren
dc.subjectX-ray diffraction analysisen
dc.titleSol-gel processing of tellurite powderen
dc.typeArticleen
dc.contributor.departmentLoughborough University. Institute of Polymer Technology and Materials Engineering.en
dc.identifier.journalJournal of Materials Scienceen
ref.citationcount1 [Scopus, 10/05/2010]en
or.citation.harvardWeng, L. Q. and Hodgson, S. N. B. (2001) 'Sol-gel processing of tellurite powder', Journal of Materials Science, 36 (20), pp.4955-4959.-
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