Hdl Handle:
http://hdl.handle.net/10149/98498
Title:
Sol-gel approach to preparing germanium disulphide
Authors:
Seddon, A. B.; Hodgson, S. N. B. (Simon); Scott, M. G.
Affiliation:
University of Sheffield. School of Materials.
Citation:
Seddon, A. B., Hodgson, S. N. B. and Scott, M. G. (1991) 'Sol-gel approach to preparing germanium disulphide', Journal of Materials Science, 26(10), pp.2599-2602.
Publisher:
Springer Verlag
Journal:
Journal of Materials Science
Issue Date:
Jan-1991
URI:
http://hdl.handle.net/10149/98498
DOI:
10.1007/BF02387724
Abstract:
A sol-gel route to germanium disulphide reported in the literature, via dihydrogen sulphide treatment of germanium tetra-ethoxide, has been re-examined. It has been found that the reported X-ray diffraction pattern of the product previously obtained coincides with germanium dioxide and not disulphide. A repetition of the synthesis, and investigation of the product by infrared spectroscopy and X-ray diffractometry, shows that germanium disulphide is indeed formed but contamination by oxide is difficult to avoid.
Type:
Article
Language:
en
Keywords:
sol-gel; germanium disulphide; germanium dioxide; X-ray diffraction
ISSN:
0022-2461; 1573-4803
Rights:
Author can archive post-print (ie final draft post-refereeing). For full details see http://www.sherpa.ac.uk/romeo/ [Accessed 11/05/2010]
Citation Count:
10 [Scopus, 11/05/2010]

Full metadata record

DC FieldValue Language
dc.contributor.authorSeddon, A. B.en
dc.contributor.authorHodgson, S. N. B. (Simon)en
dc.contributor.authorScott, M. G.en
dc.date.accessioned2010-05-11T13:24:21Z-
dc.date.available2010-05-11T13:24:21Z-
dc.date.issued1991-01-
dc.identifier.citationJournal of Materials Science; 26(10):2599-2602en
dc.identifier.issn0022-2461-
dc.identifier.issn1573-4803-
dc.identifier.doi10.1007/BF02387724-
dc.identifier.urihttp://hdl.handle.net/10149/98498-
dc.description.abstractA sol-gel route to germanium disulphide reported in the literature, via dihydrogen sulphide treatment of germanium tetra-ethoxide, has been re-examined. It has been found that the reported X-ray diffraction pattern of the product previously obtained coincides with germanium dioxide and not disulphide. A repetition of the synthesis, and investigation of the product by infrared spectroscopy and X-ray diffractometry, shows that germanium disulphide is indeed formed but contamination by oxide is difficult to avoid.en
dc.language.isoenen
dc.publisherSpringer Verlagen
dc.rightsAuthor can archive post-print (ie final draft post-refereeing). For full details see http://www.sherpa.ac.uk/romeo/ [Accessed 11/05/2010]en
dc.subjectsol-gelen
dc.subjectgermanium disulphideen
dc.subjectgermanium dioxideen
dc.subjectX-ray diffractionen
dc.titleSol-gel approach to preparing germanium disulphideen
dc.typeArticleen
dc.contributor.departmentUniversity of Sheffield. School of Materials.en
dc.identifier.journalJournal of Materials Scienceen
ref.citationcount10 [Scopus, 11/05/2010]en
or.citation.harvardSeddon, A. B., Hodgson, S. N. B. and Scott, M. G. (1991) 'Sol-gel approach to preparing germanium disulphide', Journal of Materials Science, 26(10), pp.2599-2602.-
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